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Wysłany: Nie 12:18, 13 Mar 2011
Temat postu: Well cough and cold tablets of paracetamol prime a
Well cough and cold tablets of paracetamol prime and more willing to determination of ether
200mg, more willing to ether 60mg, home 200mL volumetric flask, add the mobile phase A dissolved and diluted to the mark, shake, precise amount of l0, 20,3 O, 40,50 mL split 100mL volumetric flask,
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, diluted to use the same solvent scale, shake determination under way by the determination of a concentration as abscissa and peak area for the vertical axis, acetaminophen, and more willing to ether of linear equations in Table 1: Table 1, acetaminophen,
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, and more willing to ether linear relationship (n = 5) Tab. 1Linearcorrelationofprarcetamolandguaiphenesin good linear relationship between the old ceramic components test accurately weighed 2.4 Recovery of paracetamol reference substance about 20,
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,30,40 mg of the two, split in 100mL flask,
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, and the other more accurately weighed Gan ether 7, lO , 13mg each in duplicate, were added to the 100mL flask, each flask add blank materials 8mg, phenylephrine hydrochloride and chlorpheniramine maleate in a mixed solution (weighed phenylephrine hydrochloride 5mg, Chlorpheniramine Maleate 2mg, dissolved in mobile phase A and dilute to 100mL) 10mL ~ dissolved in mobile phase A and dilute to volume, shaken, filtered, the filtrate obtained as a continued recovery of the solution, according to assay methods under measured to calculate recovery. Of the B 1 Ye Xiangyang, et al: Happiness cough and cold tablets of paracetamol prime and more willing to determination of acyl ether 6 were average recovery of phenol 100.3%, RSD = 0.8%; more willing to ether 6 copies of the average recovery 99.5%, RSD = 0.9% 2.5 Recovery test reproducibility test obtained under which a solution of 6 successive injections of acetaminophen RSD = 0.3%, more Gan ether RSD = 0.6%, good reproducibility. 2.6 Test Stability Test 6 were obtained recovery solution, place 24h after the determination of the basic stability of the results in Table 2. Table 2 Stability Test Results Tab. 2Resultsofstabilitytests24oo227245181136514023548952476756346928782411584245061636721493545062471690446654272.7 method of determination according to the results of three batches of samples in Table 3.3 discussed and adopted a series of experiments show that this method can effectively separate the components shown in Figure 1, one can detect two components of which , the operation simple and fast, accurate and reliable for its quality control. Table 3 Determination results of samples of Tab. 3Determinationresultsofsamples1 acetaminophen more willing to ether Figure 2 1HPLC chromatogram Fig. 1HlPLCchromatogram
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